电感耦合等离子体发射光谱法测定食品中的硼酸含量.PDF

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电感耦合等离子体发射光谱法测定食品中的硼酸含量.PDF

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3 3 Vol. 3 No. 3 2012 6 Journal of Food Safety and Quality Jun. , 2012 * 刘聪祖文川汪雨 (, 100089) 摘要：目的 , 方法 , (ICP-OES) ICP-OES 结果 0.100~5.000 μg/mL , Y=63.38X +38.14, r 0.99973.54 μg/g结论 , 关键词：; ; ; Determination of boric acid in food by inductively coupled plasma-optical emission spectrometry * LIU Cong , ZU Wen-Chuan, WANG Yu (Beijing Center for Physical and Chemical Analysis, Beijing 100089, China) ABSTRACT: Objective To determine the content of boron and boric acid in food by inductively coupled plasma-optical emission spectrometry (ICP-OES). Methods The food samples were digested by the micro- wave assisted digester under a prescribed program, then the sample solution obtained was used for the ICP-OES determination of boron content. The instrument parameters of ICP-OES determination of boron were optimized. Results A good linear relationship was detected in the concentration range of 0.100~5.000 μg/mL (r=0.9997), the formula of standard curve was Y=63.38X +38.14. The detection limit of this method was 3.54 μg/g. Conclusion The described method is fast and efficient, and can be applied for boric acid determination in various foods in the market. KEY WORDS: boric acid; inductively coupled plasma-optical emission spectrometry; microwave digestion; food [2] 1 引言