对金属保护的抗刮伤、耐磨损和缓蚀有机、无机混合材料保护层.pptVIP

Experimental Details In the former case, the coated substrates were pre-dried for few minutes at environmental conditions (~20 °C and 40% HR) and subsequently baked in convection oven at 250 °C for 45 min to cross-link the polysiloxane resin.In the latter case, the organo-silane interlayers were pre-dried for few minutes at environmental conditions ($20 °C and 40% HR) and subsequently baked in convection oven at approximately 100–110 °C for 10 min to achieve the full consolidation of the primer.The organo-silane coated metal substrates were then recoated with a second layer of the polysiloxane resin. Its dring process is the same as the former case. * Experimental Details All the manufactured coatings are summarized in Table 1. Four reference samples in Fe 430 B, uncoated or Zn coated (deposited by hot dipping, cold spraying, electro-galvanizing), with layers of equivalent thickness to the above mentioned hybrid organic inorganic coatings, was used for comparative purposes. * Experimental Details Experimental procedure: Coatings thickness and their uniformity was measured by a magnetic inductive gauge,performing nine measurements equally distributed over the coated surface. Cross-cut tape test method and pencil test method were performed to evaluate the coatings adhesion to the substrate and their hardness. Coatings morphology was analyzed by contact inductive gauge of a CLI pro?ler. Stored pro?les were elaborated using theTaly Map 3.1 software, and main roughness parameters were evaluated. A Field Emission Gun – Scanning Electron Microscope was used to examine the visual appearance and morphology of the coatings. * Experimental Details Scratch tests were performed on the protective coatings, operating in “progressive load”mode,using a Rounded Conical Rockwell C diamond indenter, with 200 and 800 um tip radius. Wear endurance of the coatings was assessed by ball-on-flat linear reciprocating tribological tests,using sp