Zn_xFe_3_x_O_4纳米晶的结构及磁性.pdfVIP

研究与实验 Zn Fe － O 纳米晶的结构及磁性 x 3 x 4 吕庆荣，胡国光，方庆清，尹 平 （安徽大学物理系，安徽合肥 230039 ） 摘 要：用化学共沉淀法制备出Zn Fe － O (x =0.3～0.9)纳米铁氧体，并对其结构及磁性能进行了分析研究。 x 3 x 4 发现x=0.3～0.7 的样品为Zn 铁氧体与Fe O 双相结构，x=0.8, 0.9 的样品为单相Zn Fe － O ，晶粒尺寸均为30nm 2 3 x 3 x 4 左右。Zn Fe － O 具有亚铁磁性，样品具有较高的饱和磁化强度及较低的矫顽力。 x 3 x 4 关键词：锌铁氧体；纳米晶；化学共沉淀；结构；磁性能 + 中图分类号：TM277 .1 文献标识码：A 文章编号：1001-3830(2003)03-0017-02 The Structure and Magnetic Properties of Nanocrystalline Zn Fe － O x 3 x 4 LV Qing-rong, HU Guo-guang, FANG Qing-qing, YIN Ping Department of Physics, Anhui University, Hefei 23 0039, China Abstract ：The nanocrystalline Zn Fe － O (x=0.3 to 0.9) ferrites are prepared by chemical co-deposition method, x 3 x 4 and the structure and magnetic properties of the samples are studied. The results show that two-phase structure of Zn ferrite and Fe O can be obtained for the samples with x=0.3 to 0.7; and monophase Zn Fe － O can be obtained for the 2 3 x 3 x 4 samples with x=0.8, 0.9. The grain sizes are about 30nm. Zn Fe － O is ferromagnetic. The high σ and low H can be x 3 x 4 s c attained for all samples. Key words ：Zn ferrite; Nanocrystalline; chemical co-deposition method; st