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环糊精饱和水溶液法脱除鹿茸超临界萃取物中胆固醇的-中国管理科学
※工艺技术 食品科学 2008, Vol. 29, No. 07 179
周 冉,李淑芬*
(天津大学化工学院,绿色合成与转化教育部重点实验室,天津 300072)
:本实验以胆固醇去除率为考察指标,确定了β- 环糊精饱和水溶液包合法脱除鹿茸超临界萃取物中胆固醇
的最佳工艺,并用HPLC 法确定了萃取物中三种有效成分的保留率。实验结果表明,在β- 环糊精饱和溶液用量(ml)
与萃取物质量(mg) 比为1:2、包合温度50 ℃、包合时间为30min 、萃取物的水稀释浓度为0.8%(W/V)条件下,鹿茸
超临界萃取物中胆固醇含量可从47622.37μg/g 降低到3981.23μg/g ,脱除率高达91.64%,尿嘧啶、次黄嘌呤和尿苷
三种有效成分保留率分别为77.31% 、82.58%、85.19%,从而为鹿茸保健品及药品行业提供了安全卫生的原料基础。
:β- 环糊精;鹿茸;超临界C O 2 萃取;胆固醇
Cholesterol Removal from Supercritical Extract of Antler Velvet Using Saturated
Aqueous Solution of β-Cyclodextrin
ZHOU Ran ,LI Shu-fen*
(Key Laboratory for Green Chemical Technologies, Ministry of Education,School of Chemical
Engineering and Technology, Tianjin University, Tianjin 300072, China)
Abstract:With removal rate of cholesterol as detective index, the optimum conditions of cholesterol removal from supercritical
CO2 extract of antler velvet were confirmed using saturated water solution of β-cyclodextrin, and the retention rates of three
effective components were determined. The experimental results indicated that the content of cholesterol reduces from
47622.37 μg/g to 3981.23 μg/g, and removal rate of cholesterol is up to 91.64%, while the retention rates of three biological bases
are 77.31% ,82.58%, and 85.19%, respectively on the conditions of ratio of β-CD to the extract 1:2 (ml/mg), inclusion
temperature 50 ℃, inclusion time 30 min, and diluted concentration of the extract with water 0.8% (W/V). This process can offer
safe and health products by most of cholesterol removal from the extract of antler velvet.
Key words :β-CD ;antler velvet ;supercritical CO2 extraction ;cholestero
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