凝胶渗透色谱净化超高效液相色谱法测定辣椒油和火锅底料中的10种.PDF

6 2 Vol. 6 No. 2 2015 2 Journal of Food Safety and Quality Feb. , 2015 1 1,2 1 1 1 1 路 杨 , 杨立新 , 刘印平 , 王丽英 , 董 彬 , 常凤启 (1., 050021; 2., 100871) 摘 要: 目的 10 方法 , , 10 , 结果 , , 56.0%~96.4% 70.0%~98.2% , RSD (n=6) 1.9%~8.2% 1.8%~7.9%, (S/N=3)0.009~0.051 mg/kg , (S/N=10) 0.030~0.153 mg/kg 结论 , , 关键词: ; ; ; ; Determination of 10 dyes in hotpot material and chill by ultra performance liquid chromatography with gel permeation chromatography cleanup 1 1,2 1 1 LU Yang , YANG Li-Xin , LIU Yin-Ping , WANG Li-Ying , DONG Bin1, CHANG Feng-Qi1 (1. Hebei Center for Disease Control and Prevention , Shijiazhuang 050021, China; 2. College of Environmental Science and Engineering, Peking University, Beijing 100871, China) ABSTRACT: Objective To establish a method for the determination of 10 dyes in hot pot material and chili oil. Methods Ten dyes in chili oil, hotpot material and other foods with abundant fat were detected by gel permeation chromatography (GPC) with ultra performance liquid chromatography (UPLC). At the same time the effectiveness was verified. Result