含硫酸镁废水石灰乳法制备氢氧化镁工艺中的分析方法建立-应用化学专业论文.docxVIP

Abstract Abstract 硕士论文 Abstract In this dissertation,a systematic series of analytical methods and its application were studied，to meet the analytical requirements of improved process for preparing magnesium hydroxide from the--10％magnesium sulfate wastewater generated from the nickel producing of laterite． Based on the magnesium hydroxide preparation process，the materials were classified and summarized as raw materials，intermediate products and products．The standards of lime and calcium chloride were directly used to analyse the FaW materials． The analytical methods for the magnesium and sulfate in the magnesium hydroxide original fluid and the calcium and magnesium in four kinds of intermediate mixture， were approved via improving the sampling operating methods，SO as to adapt to the practical technology．The analytical method of the sulfate in product Was buiR based on references，since it is absence in the standard．All of these formed a set of systematic methodwhich is applied to the preparation process of magnesium hydroxide．Then,both the exactitude and accuracy of the analytic methods were studied，including the evaluation of the analytic result．In addition,the analytical methods were applied to the practical preparing process，and the suggestions for further improvement were given勰well． As a result,the standard deviations of the systematic methods were below 1％， and the recoveries were from 95％to 1 05％．Tracking analysis of preparing process and the analysis of magnesium hydroxide were tested twice，and the results were basically stable．Results of products analysis were followed：the content of Mg(OH)2 in magnesium hydroxide were 98．7％-98．8％，and the content of impurity including CaO，HCI insoluble ash,chlorides，sulfate，Fe and moisture were 0．32％-0．36％， 0．21％-O．23％， O．26-0．28％，0．34％-0