金字塔形多管微波炭化炉的研制及其应用研究-林产化学与工业.PDF

金字塔形多管微波炭化炉的研制及其应用研究 1 2 2 2 3 赵 敏 ,朱端卫 ,周文兵 ,王砚 ,孙 宇 (1.安徽师范大学环境科学与工程学院, 安徽 芜湖 241000;2.华中农业大学资源与环境学院, 湖北 武汉 430070;3.安徽省化工设计院, 安徽 合肥 230000) 摘摇 要:摇 自行设计并制造了金字塔形微波谐振腔的炭化炉,3 个微波管从3 个方向进行辐照,谐 振腔内部增加了微波搅拌器,改变了微波辐照均匀性。 双层微波防泄漏炉门设计,降低了微波泄漏 ZHAO Min摇 摇 的风险。 经过应用研究表明,微波辐照功率1160W,辐照时间18min,制得活性炭的亚甲基蓝吸附 值210mL/ g,为国家标准规定的活性炭一级品GB/ T 13803.3-1999 的1.75倍。 在680W条件下,微波辐照载苯酚废活 性炭5min,可以获得亚甲基蓝吸附值为110mL/ g 的再生活性炭,优于国家规定的二级品标准。 关键词:摇 谐振腔;微波;活性炭 中图分类号:TQ35摇 摇 摇 摇 摇 摇 文献标识码:A摇 摇 摇 摇 摇 摇 文章编号:0253-2417(2012)05-0034-07 Manufacturing and Application of Pyramid Multi鄄tube Microwave Carbonization Furnace 1 2 2 2 3 ZHAO Min ,ZHU Duan鄄wei ,ZHOU Wen鄄bing ,WANG Yan ,SUN Yu (1.College of Environmental Science and Engineering,Anhui Normal University,Wuhu241000,China; 2.College of Resources and Environment,Huazhong Agricultural University,Wuhan430070,China; 3.Chemical Engineering Design Institute of Anhui Province,Hefei230000,China) Abstract:The pyramid microwave carbonization furnace was designed and manufactured. Microwave was irradiated by three mi鄄 crowavetubefrom three directions. Thefurnacewas equippedwith a blender,which increase the uniformity in resonant cavity. The design of double microwave leakage protection furnace door reduces the risk of microwave leakage. The research results showed that under the microwave irradiation power 1 160 W and radiation time 18 min,the activated carbon has methylene blue adsorption value of210 mL/ g,which is 1.75 times higher than the specifications in the standerd of activated carbon grade A (GB/ T 13803.3-1999). Under the irradia