甲醇钠催化樟树籽仁油制备结构脂质-化学工程专业论文.docxVIP

PAGE PAGE VI Abstract Single factor experiment was used to study the effects of reaction temperature, reaction time and amount of catalyst on the transesterification reaction. On the basis of its results, orthogonal experiment was designed to ascertain the best synthesis process. The best synthesis process is as follows: the reaction temperature is 85 ℃, the reaction time is 60min, the amount of sodium methylate is 0.35%, the best ratio of raw materials is 1:1.And the crystal form of product is βwhich measured by XRD, isotherms show that the product has good compatibility, it hadn’t detected trans fatty acids in the product. Key words: camphor seed kernel oil ； soybean oil ； palm stearin; ； sodium methylate ；medium-and-long chain triacylglycerols；zero trans fatty plastic lipids；transesterification. 目录 目录 目 录 HYPERLINK \l _bookmark0 第 1 章 绪论 1 HYPERLINK \l _bookmark1 1.1 前言 1 HYPERLINK \l _bookmark2 1.2 结构脂质简介 1 HYPERLINK \l _bookmark3 1.3 结构脂质的合成方法 2 HYPERLINK \l _bookmark4 1.3.1 化学催化法 2 HYPERLINK \l _bookmark5 1.3.2 酶合成法 3 HYPERLINK \l _bookmark6 1.4 结构脂质中甘三酯组成的检测 3 HYPERLINK \l _bookmark7 1.4.1 传统方法 3 HYPERLINK \l _bookmark8 1.4.2 高效液相色谱法 4 HYPERLINK \l _bookmark9 1.5 结构脂质产品 5 HYPERLINK \l _bookmark10 1.5.1 中长碳链甘油三酯 5 HYPERLINK \l _bookmark11 1.5.2 零反式脂肪酸塑性油脂 6 HYPERLINK \l _bookmark12 1.6 国内外研究现状 7 HYPERLINK \l _bookmark13 1.6.1 中长碳链甘油三酯 8 HYPERLINK \l _bookmark14 1.6.2 零反式脂肪酸塑性油脂 9 HYPERLINK \l _bookmark15 1.7 本课题的的研究目的、意义及主要内容 10 HYPERLINK \l _bookmark16 1.7.1 课题的研究依据及意义 10 HYPERLINK \l _bookmark17 1.7.2 研究目的 11 HYPERLINK \l _bookmark18 1.7.3 研究内容 11 HYPERLINK \l _bookmark19 第 2 章 原料的制取与分析测定 12 HYPERLINK \l _bookmark20 2.1 实验材料和仪器 12 HYPERLINK \l _bookmark21 2.1.1 原料 12 HYPERLINK \l _bookmark22 2.1.2 试剂 12 HYPERLINK \l _bookmark23 2.1.3 实验仪器 12 HYPERLINK \l _bookmark24 2.2 实验方法 13 HYPERLINK \l _bookmark25 2.2.1 樟树籽仁油的制取 13 HYPERLINK \l _bookmark26 2.2.2 樟树籽仁油甘三酯的纯化 13 HYPERLINK \l _bookmark2