- 1、本文档共4页,可阅读全部内容。
- 2、原创力文档(book118)网站文档一经付费(服务费),不意味着购买了该文档的版权,仅供个人/单位学习、研究之用,不得用于商业用途,未经授权,严禁复制、发行、汇编、翻译或者网络传播等,侵权必究。
- 3、本站所有内容均由合作方或网友上传,本站不对文档的完整性、权威性及其观点立场正确性做任何保证或承诺!文档内容仅供研究参考,付费前请自行鉴别。如您付费,意味着您自己接受本站规则且自行承担风险,本站不退款、不进行额外附加服务;查看《如何避免下载的几个坑》。如果您已付费下载过本站文档,您可以点击 这里二次下载。
- 4、如文档侵犯商业秘密、侵犯著作权、侵犯人身权等,请点击“版权申诉”(推荐),也可以打举报电话:400-050-0827(电话支持时间:9:00-18:30)。
查看更多
9 2 () Vo.l 9 No. 2
2009 6 JOU RNAL OF NAN JING NORMAL UN IVERS ITY ( ENG INEERING AN D TECHNOLOGY EDIT ION ) Jun, 2009
用单月桂酸聚乙二醇山梨醇酐酯制备溶胶 凝胶
毛细管气相色谱柱及其分离能 之研究
王东新
( , 210097)
[ ] .
, : .
. 2 802 /m .
1.
[ ] , , ,
[ ] O 657. 7 [ ] B [] 2009) 02004 804
Preparation of the SolGelCapillary Column forGas Chromatography
W ith Polyoxyethylene SorbitanMonolaurate as Stationary Phase
and Separation on the Column
W ang Dongx in
( S chool of Ch em ist y and Envi onm ental S cience, Nanjing N om al Un ive s ity, N anjing 210097, C h ina)
Abstract: So lge lm e thod was used in p epa ing capilla y column w ith po lyoxye thy lene so b itan m ono lau ate as sta tiona y
phase fo g as ch om atog aphy. The g as ch om atog aphy of the so lgel column show ed ex cellent sepa ation of va ious com
pounds, inc luding nonpola and po la compounds, such as a lkanes, a om atic hyd oca bons, alcoho ls, am ines, ca boxy l
ic ac ids, phenols, este s e tc. Good epeatab ility and low baseline indicated ex cellent the m ostab ility. Sha p and na ow
peaks and the theo etica l plate num be ( 2 802 /m ) ind icated good co lumn effic iency. Symm et ic peaks and the va lue of
asymm e t ic fac to show ed good ine tness of the column.
K ey words: solge,l capilla y co lum n, gas ch om atog aphy, po lyoxye thy lene so b itan m ono lau a te
, .
, . .
[ 1]
.
[ 2] [ 3]
.
, .
1 实验部分
11
: 4890D ( FID ) ; ; 800(
); WH 2 () .
: ( 250 m i. d. , ) ; ( AR,
); ( AR, () , 5% ) ;
(); (); (
) .
:
: , , , : . Em ail: w angdongx in@ njnu. edu. cn
48
文档评论(0)