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教学要求与安排 学时:讲课20 h,上机检索和其他查阅实践10 h 教材:《化学文献检索及查阅方法》第四版,余向春编著,科学出版社 SCI或EI论文1 ~ 2篇 成绩评定: 平时10% + 期中20%(查阅文献) + 期末70% But It’s Not Google. 但它不是谷歌。 课程讲授内容 第一章、绪论 第二章、期刊 第三章、CA 第四章、SCI和EI 第五章、论文写作 第一章 第五章 第五章 第五章 3.89 90 4.51 93.5 * CC 5.33 -4.67 30 30 3.93 4.32 31.6 28.6 * * CP TC 95.9-104.1 92.0-97.8 103.6-104.4 96.7-114.0 107.5-110.7 96.4-107.2 93.9-114.6 97.3-102.1 90.4-100.8 90.3-110.6 4.00 4.00 7.5 7.5 2.88 1.16 * * 7.8 7.8 KG FP PE E PE E Recovery (%) Relative error (%) Labeled contents (mg/tablet) RSD (%) (n=5) Found contents (mg/tablet) Sample Table 2 Determination results of ephedrine and pseudo-ephedrine in the samples CONCLUSION A FIA-CE system with a simple interface based on commercial i.d. 25 μm capillary had been developed for the analysis of basic traditional Chinese medicines. The analysis of five Chinese medicinal preparations had demonstrated that the designation could produce a working device based on current chemistries and detection systems. The FIA-CE device fabricated out of organic glass base and an i.d. 25 μm commercial capillary and used both electro-kinetic and electro-osmotic flow techniques to facilitate the mixing and mobility of reagents and samples. Such designation strategies have two advantages: one is to get any micrometer-sized micro-channel from commercial capillaries including rectangle micro-channel of higher aspect ratio (Giddings et al., 1983); the other is characteristics of tractability of organic glass to overcome disadvantages of geometry limited in planar structure of photolithography (Xia and Whitesides , 1998), despite of the some shortcomings in its rollout (Fang and Fang, 2001). The separation and determination of ephedrine and pseudo-ephedrine was selected as a well-understood process with which to evaluate the FIA-CE methodology. A more fundamental study of optimum conditions in hybrid device of FIA and CE has yet to be concluded, but the initial results from this and
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