冷饭团花及果实挥发性成分鉴定.doc

冷饭团果实挥发性成分鉴定与分析 高渐飞1 ,，杨 艳2基金项目：贵州省科技支撑计划项目：贵州省珍稀植物冷饭团种植资源调查收集、保护、驯化栽培技术示范研究(黔科合字[2013]3173号)? 基金项目：贵州省科技支撑计划项目：贵州省珍稀植物冷饭团种植资源调查收集、保护、驯化栽培技术示范研究(黔科合字[2013]3173号)? 第一作者简介：高渐飞(1985-)，男(汉族)，贵州威宁人，硕士，助理研究员，主要从事生态治理与植物资源开发，E-mail： gaojf2010@163.com. *通讯作者：杨艳.E-mail: yishideyangzi@163.com （1.贵州省山地资源研究所,， 贵州 贵阳 550001；2.贵州省中国科学院天然产物化学重点实验室,， 贵州 贵阳 550002；3.贵州工业职业技术学院，贵州 贵阳 550008） 摘要：为研究明确冷饭团（Kadsura Coccinea）果实部分挥发性成分及含量。，以其花、果皮、果肉、籽为材料，采用顶空-固相微萃取与气相色谱-质谱联用技术，对果实不同部位的挥发性有机成分进行了研究。结果显示：4个部位鉴定出94种化合物，含量为92.8%；，不同部分释放物质类型及含量存在差异性，但均含有醇、烷、烯类物质，亦是等主要构成种类成分，其中又以烯类为主；4个部位监测到6种共同含的化合物，但都不是主要构成成分。冷饭团花、果肉、果皮主要挥发性成分有石竹烯、蒎烯、大月桂烯、榄香烯、毕澄茄烯等，它们大部分具有保健和药用的功效。 关键词：冷饭团；果实；挥发油；GC-MS Identification and Analysis of Volatile Compounds of Kadsura Coccinea Fruit Abstract: Volatile compounds of Kadsura Coccinea fruit was analyzed and studied. Flower, skin, flesh and seed of Kadsura Coccinea fruit were extracted (and analyzed) using solid phase micro extraction (SPME) and gas chromatography-mass spectrometry (GC-MS). The result showed that 94 compounds were identified from 4 parts of Kadsura Coccinea fruit and content of which was 92.8%. Through release (identification) of substances to species, alcohols, alkanes and alkenes were the major compounds. Alkenes were the most major compounds. There were differences of compounds from 4 parts of Kadsura Coccinea fruit and the main components were not the same. 4 parts of Kadsura Coccinea fruit contained 6 same kinds identical compounds, but which were not major component. There were differences from content and material types of 4 parts of Kadsura Coccinea fruit; however 4 parts of Kadsura Coccinea fruit all contained 3 kinds main constituent substances such as alcohols, alkanes and alkenes and alkenes were the most major constituent substances. Caryophyllene, Pinene, Myrcene and Cadinene were major compounds of flower, skin and flesh of Kadsura Coccinea fruit, which had health and medicinal effects. Key Word: Kadsura coccinea; distillation method