Silicalite-1分子筛氢键诱导晶化机制的固体核磁共振研究.PDFVIP

Supporting Information for Acta Phys. -Chim. Sin. doi: 10.3866/PKU.WHXB201905035 Silicalite-1 分子筛氢键诱导晶化机制的固体核磁共振研究 1,2 1 1 1,* 1,* 刘小龙 ，王强 ，王超 ，徐君 ，邓风 1 中国科学院武汉物理与数学研究所，波谱与原子分子物理国家重点实验室，武汉磁共振中心，中国科学院生物磁共振重点 实验室，武汉 430071 2 中山大学材料学院，广州 510275 Hydrogen-Bond Induced Crystallization of Silicalite-1 Zeolite as Revealed by Solid-State NMR Spectroscopy 1,2 1 1 1,* 1,* LIU Xiaolong , WANG Qiang , WANG Chao , XU Jun , DENG Feng 1 State Key Laboratory of Magnetic Resonance and Atomic and Molecular Physics, Wuhan National Center for Magnetic Resonance, CAS Key Laboratory of Magnetic Resonance in Biological System, Wuhan Institute of Physics and Mathematics, Chinese Academy of Sciences, Wuhan 430071, P. R. China. 2 School of Materials, Sun Yat-Sun University, Guangzhou, 510275, P. R. China. * Corresponding authors. Emails: xujun@wipm.ac.cn (X.J.); dengf@wipm.ac.cn (D.F.). Tel.: +86-27 s1 Fig. S1 XRD patterns of as-synthesized samples heated at 180 °C for different time. 20 h 18 h 16 h 15 h 5 h 0 h Fig. S2 SEM images of as-synthesized samples heated at 180 °C for different time. s2 Fig. S3 1H DQ-SQ (right) NMR spectra of as-synthesized samples heated at 180 °C for (a