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handout synthesis of salicylic acid - 3：讲义合成水杨酸-
Section
GTA
Station
8.Synthesis
of
Salicylic
Acid
Pre-lab
questions
Complete
the
following
questions.
Show
all
work.
All
work
and
answers
must
be
typed.
1.
How
many
moles
of
methyl
salicylate
are
you
using
in
this
reaction?
2.
What
is
the
minimum
number
of
moles
of
sodium
hydroxide
needed
to
insure
complete
deprotonation
of
the
methyl
salicylate
in
question
#1?
3.
How
many
moles
of
sodium
hydroxide
(NaOH)
will
be
used
in
your
experiment?
4.
How
many
millileters
(mL)
of
the
sulfuric
acid
solution
should
be
added
to
insure
complete
protonation
of
the
intermediate?
5.
Assume
you
recover
1.1
g
of
product
after
recrystallization.
What
is
your
%
yield?
8.Synthesis
of
Salicylic
Acid
Jones:Ester
hydrolysis,
saponification
pg
955,
Figure
19.33
McMurry:Ester
hydrolysis,
saponification
pgs
325-326
Vocabulary:Theoretical
yieldThe
yield
of
a
reaction
assuming
100%
conversion
of
the
limiting
reagent
to
the
product.
Limiting
reagent
The
reagent
which
is
present
in
the
smallest
amount
and
would
limit
the
amount
of
product.
ReagentA
compound
which
is
used
as
the
starting
material
for
a
reaction.
This
procedure
has
been
adapted
from
the
microscale
procedure
described
in
Experimental
Organic
Chemistry
A
Balanced
Approach:
Macroscale
and
Microscale
by
Jerry
R.
Mohrig,
Terrence
C.
Morrill,
Christina
Noring
Hammond,
and
Douglas
C.
Necke
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