标准、规范、准则_EPA Method 605 Benzidines.pdf

APPENDIX A TO PART 136 METHODS FOR ORGANIC CHEMICAL ANALYSIS OF MUNICIPAL AND INDUSTRIAL WASTEWATER METHOD 605—BENZIDINES 1. Scope and Application 1.1 This method covers the determination of certain benzidines. The following parameters can be determined by this method: Parameter Storet No. CAS No. Benzidine . . . . . . . . . . . . . . . . . . . . . 39120 92-87-5 3,3-Dichlorobenzidine . . . . . . . . . . . . 34631 91-94-1 1.2 This is a high performance liquid chromatography (HPLC) method applicable to the determination of the compounds listed above in municipal and industrial discharges as provided under 40 CFR Part 136.1. When this method is used to analyze unfamiliar samples for the compounds above, identifications should be supported by at least one additional qualitative technique. This method describes electrochemical conditions at a second potential which can be used to confirm measurements made with this method. Method 625 provides gas chromatograph/mass spectrometer (GC/MS) conditions appropriate for the qualitative and quantitative confirmation of results for the parameters listed above, using the extract produced by this method. 1 1.3 The method detection limit (MDL, defined in Section 14.1) for each parameter is listed in Table 1. The MDL for a specific wastewater may differ from those listed, depending upon the nature of the interferences in the sample matrix. 1.4 Any modificatio