乳液微封装技术制备聚苯乙烯空心微球PREPARATIONOF.pdfVIP

CNIC-01672 CAEP-0134 乳液微封装技术制备聚苯乙烯空心微球 PREPARATION OF POLYSTYRENE MICROSPHERE WITH EMULSION MICROENCAPSULATION METHOD (In Chinese) 中 国 核 情 报 中 心 China Nuclear Information Centre 79 CNIC-01672 CAEP-0134 乳液微封装技术制备聚苯乙烯空心微球 李 波 张 林 张占文 游 丹 魏 芸 王朝阳 林 波 师 涛 初巧妹 （中国工程物理研究院激光聚变研究中心，绵阳，621900 ） 摘 要 介绍了乳液微封装技术制备不同直径空心聚苯乙烯微球的工艺 技术，着重研究了表面活性剂、电解质、水溶性聚合物对多重乳液 的稳定性、微球的直径以及微球表面光洁度的影响。在选定的实验 参数下，制备得到直径 150～3000 µm ，壁厚 0.8～15 µm ，表面粗糙 度 Ra 约为 4 nm ，微球同心度≥95%的空心聚苯乙烯微球。 关键词：微封装 聚苯乙烯 微球 分类号：TL62; TL67 80 Preparation of Polystyrene Microsphere with Emulsion Microencapsulation Method (In Chinese) LI Bo ZHANG Lin ZHANG Zhanwen YOU Dan WEI Yun WANG Chaoyang LIN Bo SHI Tao CHU Qiaomei (Laser Fusion Research Center, China Academy of Engineering Physics, Mianyang, Sichuan, 621900) ABSTRACT The preparation of hollow polystyrene microspheres that are used as inner shell of multi-shell plastic microspheres in the ICF experiments is focused on. The effects of surfactants, water-soluble polymer and electrolyte on the properties of resultant microspheres are studied. Based on these experiments, a fabricating procedure was established with which hollow microspheres were prepared with diameter about 150～3000 µm, wall thickness 0.8～15 µm and toughness Ra less than 4 nm. Key words ：：Microencapsulation, Polystyrene, Microsphere ：： Category