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49.7.03 0.009M H2SO4 as solvent blank. Calculate molar absorptivity (ε) at
AOAC Official Method 2000.02 each concentration as follows:
Patulin in Clear and Cloudy Apple Juices
and Apple Puree
ε
Liquid Chromatographic Method
First Action 2000
where A = absorbance at maximum near 350 nm, C = mM concentra-
(Applicable to determination of patulin at >25 ng/g in clear apple
tion of K Cr O solution.
juice, cloudy apple juice, and apple puree.) 2 2 7
If the 3 values vary by more than guaranteed accuracy of A scale,
See Table 2000.02 for results of the interlaboratory study support- check either technique or instrument. Average 3 ε values to obtain εε .
ing the acceptance of the method. Determine correction factor (CF) for particular instrument and cells
by substituting in equation:
A. Principle
Apple juice or puree is extracted with ethyl acetate and then
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