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METHOD 3570
MICROSCALE SOLVENT EXTRACTION (MSE)
1.0 SCOPE AND APPLICATION
1.1 Method 3570 is a procedure for extracting volatile, semivolatile, and nonvolatile
organic compounds from solids such as soils, sludges, and wastes. The microscale approach
minimizes sample size and solvent usage, thereby reducing the supply costs, health and safety
issues, and waste generated.
1.2 This method has been validated for several mono- and poly-cyclic aromatic
hydrocarbons (MAHs and PAHs) and can be applied to any combination of these compounds.
1.3 This method also may be used to extract any volatile organic compounds (VOCs) or
semivolatile organic compounds (SVOCs) once their extraction performance has been
demonstrated to be satisfactory using an appropriate analytical technique. Method 3570 is not
amenable to samples that have been preserved in the field using methanol.
1.4 Prior to employing this method, analysts are advised to consult the base method for
each type of procedure that may be employed in the overall analysis (e.g., Methods 3500, 3600,
5000, and 8000) for additional information on quality control procedures, development of QC
acceptance criteria, calculations, and general guidance. Analysts also should consult the
disclaimer statement at the front of the manual and the information in Chapter Two for guidance on
the intended flexibility in the choice of methods, apparatus, materials, reagents, and supplies, and
on the responsibilities of the analyst for demonstrating that the techniques employed are
appropriate for the analytes of interest, in the matrix of interest, and at the levels of concern.
In addition, analysts and data u
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