碳基光催化剂的制备及其催化性能研究.pdfVIP

制备的ZnO/碳化树脂复合物。本章研究了真空煅烧环境下不同煅烧温度、不同煅 烧时间制备的ZnO/碳化树脂复合物对甲基橙溶液降解效果，结果表明：当ZnO/ 碳化树脂复合物真空煅烧温度为380℃，煅烧时间为4h 时，光催化效果最好，在 2h 83.2% 2h 紫外光下对甲基橙溶液 脱色率可以达到 ，在可见光下对甲基橙溶液 脱色率可以达到18.6%。 3）以Zn(OH)2 碳微球为模板，采用水热合成和碳化等方法制备了ZnO/碳微球 复合物，采用扫描电子显微镜、X-射线衍射仪等手段对其进行了表征。研究了不 同方法制备的ZnO/碳微球复合物对甲基橙溶液的光催化效果的影响，结果表明真 空煅烧制备的ZnO/碳微球复合物对甲基橙溶液降解效果上要好于通氮气保护制备 的ZnO/碳微球复合物。研究了真空煅烧条件下不同煅烧温度、不同煅烧时间制备 的ZnO/碳微球复合物对甲基橙溶液降解效果，结果表明当ZnO/碳微球复合物真空 350 4h 煅烧温度为 ℃，煅烧时间为 时，在紫外光下对甲基橙溶液降解效果最好， 对甲基橙溶液2h 脱色率可以达到77.8%；然而当煅烧温度为380℃时，在可见光 2h 13.9% 下光催化效果最好，对甲基橙溶液 脱色率可以达到 。 Ag/ ZnO/ ZnO/ 关键词： 碳化树脂； 碳化树脂； 碳微球；光催化 II ABSTRACT With the acceleration of the global industrialization process, the problem of environmental pollution has become increasingly serious, and environmental governance hasreceived widespread attention from countries around the world.Among them, the government has devoted huge human, material and financial resources to the research and development of environmental purification materials and technologies industrialization provides support, of which photocatalytic materials and photocatalytic technology occupy an important position. Photocatalytic technology has become the most anticipated new technology in environmental protection because of its minimum cost, relatively stable conditions and obvious improvement in degradation.At present, the scale of catalyst preparation methods and related studies have shown that various carbonization techniques can be used to prepare catalysts with excellent performance. Carbonation referstotheprocessof dehydration of organicmatter into carbon materials, carbon-forming materials or c