年产500t环戊酮生产工艺设计(1).docxVIP

分 类 号： 密级： 学校代码： 10414 学号： 402017160012 硕士专业学位研究生学位论文 年产 500 t 环戊酮生产工艺设计 Technological design of cyclopentanone with 500 t/a 年产 年产 500 t 环戊酮生产工艺设计 PAGE \* ROMAN I PAGE \* ROMAN I 摘 要 环戊酮是一种重要的精细化工中间体，可用于制备二氢茉莉酮酸甲酯、白兰酮、2-正己基环戊酮、杀虫剂、除草剂等产品，也可用于合成抗焦虑药盐酸丁螺环酮等药物。 本设计是对年产 500 吨环戊酮生产项目进行的工艺生产设计。本设计的合成路线采用己二酸为原料，以氢氧化钠为催化剂合成环戊酮。原料经过化料、热解反应、碱洗、水洗、脱水、精馏等工序，得到高纯度的环戊酮产品。该工艺每年消耗己二酸 1010 t、氢氧化钠 15 t，最终得到环戊酮 504.9 t，环戊酮的产率为86.8%。 本设计主要包含以下设计内容：环戊酮的简介、项目背景及设计依据；环戊酮的生产工艺方案及工艺流程设计；环戊酮生产过程中主要工艺过程的物料衡算和能量衡算；主要设备选型及计算；环戊酮生产车间设备布置设计及安全生产设计等内容。 关键词：环戊酮；己二酸；工艺；设计 工程硕士专业学位论文 工程硕士专业学位论文 PAGE \* ROMAN II PAGE \* ROMAN II Abstract Cyclopentanone is an important fine chemical intermediate. It can be used to prepare methyl dihydrojasmonate, leukonone, 2-n-hexylcyclopentanone, insecticides, herbicides and other products. It can also be used to synthesize buspirone hydrochloride which is a kind of anxiolytics. This design is a process production design for a 500-ton-per-year cyclopentanone production project. The synthetic route of this design uses adipic acid as raw material and sodium hydroxide as catalyst to synthesize cyclopentanone. The raw material through the processes of melting, pyrolysis, alkaline washing, water washing, dehydration, rectification, etc. finally, a high-purity cyclopentanone products is obtained. This process consumes 1010 tons of adipic acid and 15 tons of sodium hydroxide annually, and finally obtains 504.9 tons of cyclopentanone, and the yield of cyclopentanone is 86.8%. This design mainly includes the following design contents: the introduction of cyclopentanone, project background and design basis; production process plan and process design of cyclopentanone; material balance and energy balance of the main process during cyclopentanone production; Selection and calculation of main equipment; equipment layout design and safety production design of cyclopentanone production workshop. Key words: cyclopentanone; adipic acid; technology; design 年产 年产 5