高效液相色谱法测定土壤中的二氯喹啉酸.pdfVIP

高效液相色谱法测定土壤中的二氯喹啉酸 陈虹;钟明;唐昊冶;韩勇;靳伟 【摘要】Quinclorac is an effective herbicide commonly used in rice plantation. But Quinclorac residue in soil probably brings teratogenesis to some Quinclorac sensitive rotation crops, like Solanaceae plants, Leguminosae emblements. So the residue in soil should be accurately detected. Quinclorac residue in soil sample was extracted on a to-and-fro shaker for 2 hours with 50 ml extractant, which was the mixture of methanol and 0.05 mol/L borax solution (pH = 10) at the ration of 9 ︰1 (v/v). The extracts was centrifuged and subsequently fil