SAE-ARP1313-REV.B-中文版完整版.doc

Determination of Trace Elements in High Temperature Alloys 高温合金中痕量元素的测定 1. SCOPE: 范围 This SAE Aerospace Recommended Practice (ARP) describes procedures for solution and solid graphite furnace atomic absorption spectrometric determination of lead, bismuth, selenium, tellurium, and thallium in nickel and cobalt high temperature alloys. Other analytical methods are able to provide the required accuracy and are mentioned herein. 本SAE航天推荐准则（ARP）描述了溶液和固体石墨炉原子吸收光谱法测定镍基和钴基高温合金中铅，铋，硒，碲，铊的解决方案。本文中也提到了能够提供所要求的精度的其他分析方法。 2. APPLICABLE DOCUMENTS: 适用文件 The following publication forms a part of this specification to the extent specified herein. The latest issue of SAE Publications shall apply. 下列出版物构成本规范的一部分。适用于最新一期的SAE出版。 2.1 SAE Publications: SAE出版 Available from SAE, 400 Commonwealth Drive, AMS 2280 Trace Element Control, Nickel Alloy Castings 2.2 The following literature is cited as background on the development of the analytical procedures described herein: 引用了下列文献作为分析程序的发展背景 2.2.1 Background Correction Techniques: 背景校正技术 Slavin, W., Carnick, G.. R., CRC Critical Rev. Anal. Chem. 19 (1988) 95-134 2.2.2 Solution GFAAS Method: 溶液GFAAS方法 Welcher, G. G., Kriege, O. H., Marks, J. Y., Anal. Chem. 46 (1974) 1227-1231 Sotera, J. J., Cristiano, L. C., Conley, M. K., Kahn, H. L., Anal. Chem. 55 (1983) 204-208 2.2.3 Solid GFAAS Method: 固体GFAAS方法 Marks, J. Y., Welcher, G. G., Spellman, R. J., “Applied Spectroscopy” 31(1977) 9-11 Irwin, R., Mikkelson, A., Michel, R. G., Dougherty, J. P., Preli, F.R., Spectrochim Acta, Part B” 45B (1990)903-915 3. DISCUSSION 讨论 A variety of spectroscopic and spectrometric techniques have been found to be satisfactory for determining trace quantities of deleterious elements at levels prescribed by AMS 2280. Graphite furnace atomic absorption spectrometry (GFAAS) is currently the most widely practiced technique for this application. The acid dissolution GFAAS procedure is well suited to routine bulk analysis and the solid GFAAS method can be used for rapid