γ-AlON透明陶瓷制备及稀土掺杂的上转换发光的中期报告.docxVIP

γ-AlON透明陶瓷制备及稀土掺杂的上转换发光的中期报告 中文摘要： 本项目旨在制备透明陶瓷材料γ-AlON，并通过稀土掺杂实现上转换发光。首先，通过真空烧结法制备出γ-AlON陶瓷样品，并通过XRD和SEM等手段对其进行表征。结果表明，样品为高纯γ-AlON陶瓷，晶粒尺寸为1-2μm左右，表面平整，无明显的烧结缺陷和孔洞。然后，采用化学共沉淀法对γ-AlON陶瓷进行稀土掺杂，掺杂量为2mol%。最后，利用激光器作为激发光源，测量了样品在不同激发光功率下的发光光谱，并观察到了明显的上转换发光峰，证明稀土掺杂成功。 英文摘要： The aim of this project is to prepare translucent ceramic material γ-AlON and achieve upconversion luminescence by rare earth doping. Firstly, γ-AlON ceramic samples were prepared by vacuum sintering method, and characterized by XRD and SEM. The results show that the sample is highly pure γ-AlON ceramic with a grain size of about 1-2 μm, a smooth surface, and no obvious sintering defects and pores. Then, the γ-AlON ceramics were doped with rare earth by chemical coprecipitation method, and the doping amount was 2 mol%. Finally, using a laser as the excitation light source, the emission spectrum of the sample under different excitation light powers was measured, and a significant upconversion luminescence peak was observed, indicating the successful rare earth doping.