ASTM D1996-97 美国材料与试验协会标准.pdfVIP

Designation:D1996–97(Reapproved2003)

StandardTestMethodfor

DeterminationofPhenolicAntioxidantsandErucamideSlip

AdditivesinLowDensityPolyethyleneUsingLiquid

Chromatography(LC)1

ThisstandardisissuedunderthefixeddesignationD1996;thenumberimmediatelyfollowingthedesignationindicatestheyearof

originaladoptionor,inthecaseofrevision,theyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.A

superscriptepsilon()indicatesaneditorialchangesincethelastrevisionorreapproval.

1.Scope*3.1.2BHT—2,6-di-t-butyl-4-methylhydroxybenzeneorbu-

1.1Thistestmethoddescribesaliquidchromatographtylatedhydroxytoluene.

procedurefortheseparationofsomeadditivescurrentlyused3.1.3Irganox1010—tetrakis[methylene(3,5-di-t-butyl-4-

inlowdensitypolyethylene.Theseadditivesareextractedwithhydroxyhydrocinnamate)].

2-propanolpriortoliquidchromatographicseparation.The3.1.4Irganox1076—octadecyl3-(3,5-t-butyl-4-

ultravioletabsorbance(200nm)ofthecompound(s)ismea-hydroxyphenyl)propionate.

sured;quantitationisperformedusingtheinternalstandard3.1.5Isonox129—2,2-ethylidenebis(4,6-di-t-butylhy-

method.droxybenzene).

1.2Thisstandarddoesnotpurporttoaddressallofthe3.1.6Kemamide-E—cis-13-docosenamide,erucamide.

safetyconcerns,ifany,associatedwithitsuse.Itisthe3.1.7LC—liquidchromatography.

responsibilityoftheuserofthisstandardto