粉末衍射法晶体结构测定概述.pptVIP

高质量衍射数据Accuracyof±0.02°(2-theta).MinimalFWHM=0.14to0.20°(2-theta)maysuffice.MinimalFWHMloweredto0.08-0.04°(2-theta)with correctsetofslits.Kalpha-1isbetterbutKalpha-1,2workstoo.Countingstepshouldbeaslowas0.02-0.01°(2-theta).AllispossibleonaconventionalX-raypowder diffractometer.

SynchrotroncandofarbetterwithFWHMsaslowas 0.008°(2-theta).第30页，课件共78页，创作于2023年2月高质量衍射数据Neutronpowderdiffractometerscannotoffercomparable performances.

MinimalFWHMsarenearof0.12or0.20oreven 0.30°(2-theta)dependingontheinstrument