JEOL JEM1400-Plus用户手册指南.pdf

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OperatingtheJEOLJEM1400-PlusTransmissionElectronMicroscope

ElectronMicroscopyCoreLaboratory,UniversityofUtah

FollowtheproceduresbelowwhenyouusetheJEM1400-PlusTEM.

StartingSession

1.Ifnotloggedin,logintotheuseraccountsontheJEOLandGatancomputers.(Usekeyboardandmouse

lyingontopofGatancomputertologintothatcomputer.)Afterthis,thecomputersshouldbecontrollableby

JEOLmouseandkeyboard.Ifnot,checkthatSynergyisrunningonbothmachines.

2.Checkthatthegunandcolumnvacuumisreasonable(PenningGauge30andVacReady,otherchambers

exceptspecimenchambershouldsayEvacReady).Usevalve/vacuummonitorpanel.

3.Ifthehightensionisoff,turniton.Itshouldbesetto120kV(lowerifadifferentvalueisdesired).

-Usebeamcontroller

-Ifhightensionshutsoffasyoubringupthevoltage,raisevoltagetoapointlowerthanwherethehightension

failed.Letvoltagestaythereforafewminutes.Then,bringuphightensionslowly.Forexample,turn

voltageto100kVwithbeamcontroller,thenuseHTSchedulingtogofrom100−120kVin0.1kVstepsof

onesecond.

4.Addliquidnitrogentothecoldtrap.

-RemoveACD(anti-contaminationdevice)attachmentifpresent.

-Testifconnectionsareokaybypushing(up)switchattopofdewar(belowamberlight).Ifamberlight

changescolor,thendontaddnitrogenandnotifyEMLabstaff.Thisindicatesaconductivityproblemwiththe

microscope.Ifthisoccurswhenyouhaveaddednitrogen,alsonotifystaff.

-Useafunneltoaddnitrogen.

-Addmorenitrogenduringyoursessionasneeded(e.g.hourlyorduringspecimenexchanges).

5.Aperturesettings

-condenserapertureshouldbeIN(adjustwithlever;leftisin,rightisout).

-objectiveapertureshouldb

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