pulse程序顺序cbcanhbruker topspin说明书seqcbcanh.pdfVIP

PulseProgramCatalogue

NMRGuide4.0

3DSequentialCBCANHusingTROSY(seqtrcbcanhgp3d|SEQTRCBCANHGP3D)

1121

JHC+JCACB+JNCA+JHNseqCBCANH

HCHHCH

NCCNCC

OO

HHHH

1234

HACACANNH

HBCBt2t3

t1

d26=1/4J(NH)=2.3m

N)

d21=1/4J(NCA)=12.4m

4N

d22=1/8J(CACB)=3.6m

A

d27=1/4J(NCA)=11m

4N

d24=1/4J(CACO)=4.5m

44

d4=1/4J(CH)=1.7m

4

d3=1/6J(CH)=1.1m