Ti诱导无压浸渗法制备Fe-Si基SiC陶瓷复合材料.pdfVIP

HotWorkingTechnology201Vol.47,No.24

Ti诱导无压浸渗法制备Fe-Si基

SiC陶瓷复合材料

梁朝i,刘海云气郭俊杰气孟庆森“

(1.太原理工大学材料科学与工程学院，山西太030024;2.太原理工大学新材料界面科学与工程教育部重点实

验室，山西太030024)

摘要：通过掺杂活性元素Ti颗粒，采用无压浸渗法制备了SiC/Fe-Si复合材料。采用XRD、SEM以及EDS等技

术手段，分析复合材料的相组成及显微结构。结果表明：Fe-Si合金能够自发浸渗SiC陶瓷预制体,Ti元素在金属熔体与

陶瓷颗粒之间形成活性层，促进熔融金属润湿陶瓷，诱发界面反应的发生，形成自发浸渗。在自发浸渗过程中界面反应

和元素相互扩散，导致复合材料的相组成和显微结构发生变化。

关键词：无压浸渗；SiC陶瓷;Fe-Si合金；界面反应；Ti颗粒

DOI:10.14158/j.cnki.1001-3814.20124.024

中图分类号:TB333.13文献标识码：A文章编号：1001-3814(2018)24-0098-04

PreparationoSiCCeramics/Fe-SiAlloyComposites

byTi-ActivatedPressurelessInflltration

LIANGChao,LIUHaiyun12,GUOJunjie,MENGQingsen

(1.SchoolofMaterialsScienceandEngineering,TaiyuanUniversityofTechnology,Taiyuan030024,China;2.KeyLaboratoryof

InterfaceScienceandEngineeringinAdvancedMaterials,MinistryofEducation,TaiyuanUniversityofTechnology,Taiyuan

030024,China)

Abstract:SiC/Fe-SicompositeswerepreparedbydopingactiveelementTiparticlesbypressurelessinfiltrationmethod.

ThephasecompositionandmicrostructureofthecompositeswereanalyzedbymeansofXRD,SEMandEDS.Theresults

showthat,theFe-SialloycanspontaneouslyinfiltrateSiCceramicpreform.Theactivelayerbetweenmetalmeltandceramic

particlesisformedbyTielementaddition,whichpromotesthewettingofmoltenmetaltoceramics,inducestheoccurrenceof

interfacereactionandformsspontaneousinfiltration.Intheprocessofspontaneousinfiltration,thephasecompositionand

microstructureofthecompositeschangeduetotheinterfacialreactionandthemutualdiffusionofelements.

Keywords:pressurelessinfiltration;SiC