直接熔化制备Al-Si-Al_(2)O_(3)复合材料的组织和性能.docxVIP

2024年第53卷第16期

Vol.53No.162024

热加工工艺

HotWorkingTechnology

ISSN1001-3814CN61-1133/TG

DOI:10.14158/j.cnki.1001-3814. rjggy@

直接熔化制备Al-Si-Al2O3复合材料的

组织和性能

赖旭平1,李天方1,刘瑞2,孙红亮2

(1.海军装备部,四川成都610036;2.西南交通大学材料科学与工程学院,四川成都610031)

摘要院采用光学显微尧XRD尧SEM和EDS分析了Si含量分别为10.00wt%尧7.64wt%的Al-Si-Al2O3复合材料的显微组织形貌以及物相组成遥结果表明院Al-10.00wt%Si试样的组织细小袁孔隙率较高遥基体晶粒Al呈细小圆形袁Si颗粒主要在基体晶界周围聚集长大袁部分向基体晶粒内部生长曰而Al-7.64wt%Si试样组织略微粗大袁孔隙率较低遥基体晶粒Al呈不规则形状袁Si颗粒聚集长大现象更为明显遥原位反应成功进行袁Al-10.00wt%Si复合材料以Al为基体生成的Al2O3是增强相曰另一生成物Si没有细小弥散的分布于Al基体中袁而是聚集附着在基体Al晶界周围袁且有部分SiO2残留存在于基体晶界周围遥在加热升温过程中袁混合原料只出现了部分熔化现象袁金属液滴从混合原料中析出袁凝结为含Al量极高的合金液滴遥合金液滴致密度较高袁固溶体呈枝晶状袁Si呈条状或针状曰且有小颗粒第二相的存在袁含有Al尧Si尧C元素遥

关键词院直接熔化曰感应加热曰显微组织曰Al-Si-Al2O3复合材料

中图分类号院TB333.1+2 文献标识码院A 文章编号院1001-3814(2024)16-0134-03

MicrostructureandPropertiesofAl-Si-Al2O3CompositesPreparedbyDirectMelting

LAIXuping1,LITianfang1,LIURui2,SUNHongliang2

(1.NavalEquipmentDepartment,Chengdu610036,China;2.SchoolofMaterialsScienceandEngineering,SouthwestJiaotongUniversity,Chengdu610031,China)

Abstract院ThemicrostructureandphasecompositionofAl-Si-Al2O3compositewithSicontentof10.00wt%,7.64wt%were

analyzedbyopticalmicroscopy,XRD,SEMandphaseanalysis.TheresultsshowthatthemicrostructureoftheAl-10.00wt%Sisampleisfineandtheporosityishigh.ThegrainAlofthematrixisfineandround,andtheSiparticlesmainlyaggregateandgrowaroundthegrainboundaryofthematrix,andpartlygrowintothegraininteriorofthematrix.However,themicrostructureofAl-7.64wt%Sisampleisslightlycoarseandtheporosityislow.ThegrainAlofmatrixisirregular,thephenomenonofSigrainaggregationismoreobvious.Theinsitureactioniscarriedoutsuccessfully,theAl2O3oftheAl-10.00wt%SicompositeformedbytheAlmatrixisthereinforcedphase.TheotherlifetimeSidoesnotdistributeintheAlmatrix,butaggregatesaroundtheg