石墨烯-铜复合粉体制备工艺研究.pdfVIP

HotWorkingTechnology2019,Vol.48,No.8

石墨烯-铜复合粉体制备工艺研究

张会关彤

,

陕西理工大学材料科学与工程学院陕西汉中

(,723001)

摘要：采用化学还原法，以氧化石墨烯和硫酸铜作为原材料，水合肼为还原剂，通过离心、干燥制备出石墨烯铜

-

纳米粉体。采用单一变量法，即氧化石墨烯为定量，硫酸铜为变量，通过不同的配比制备出石墨烯铜复合纳米粉体。通

-

过XRD、SEM表征分析，结果表明：当氧化石墨烯与硫酸铜满足质量比为1∶4时，混合粉体中石墨烯和纳米铜包裹最

好，且铜颗粒均匀分布在石墨烯层的周围。

关键词：石墨烯；石墨烯铜纳米粉体；；

-XRDSEM

DOI:10.14158/j.cnki.1001-3814.2019.08.031

中图分类号：+文献标识码：文章编号：

TB333.12A1001-3814(2019)08-0128-04

StudyonPreparationProcessofGraphene-copperCompositePowder

ZHANGHui,GUANTong

(SchoolofMaterialsScienceandEngineering,ShaanxiUniversityofTechnology,Hanzhong723001,China)

：

AbstractByusinggrapheneoxideandcoppersulfateasrawmaterials,hydrazinehydrateasreducingagent,the

graphene-coppernano-powderaspreparedaftercentrifugationanddryingbychemicalreductionmethod.The

graphene/coppercompositenano-powderswerepreparedbysinglevariablemethod,thatis,grapheneoxideasquantification

andcoppersulfateasvariable.TheresultsofXRD,SEMcharacterizationshowthat,whenthemassratioofgrapheneoxideto

coppersulfateis1∶4,thegrapheneandnano-copperinthemixedpowderarethebest.TheCuareparticlesdistributed

uniformlyaroundthegraphenelayer.