中科大无机非金属材料测试方法课件01 X射线粉晶衍射分析.pptVIP

FewithoutNifilter?T=90.25?FeS,SG=Th6-Pa3a=5.4176-710?NodIhkl13.12930111β22.86910011132.73120200β42.4778020051.7494022161.4945031171.43110222????81.1341033191.10620420101.0505230111.01020422FewithoutNifilterT=90.32Pb,SG=Oh5-Fm3ma=4.95066-640(?)?FewithoutNifilterT=90.32Pb,SG=Oh5-Fm3ma=4.95066-640(?)（4）依公式求出所有线条的布拉格衍射角：θ=45M/L（低角区）θ=90-45M/L（高角区）（5）求得sinθ及d值和sin2θ。（6）将各线指标化。（7）计算点阵常数。编号低角区高角区m1m2m1m2m1+m2m1-m2∑(m1+m2)∑(m1+