咪鲜胺及其代谢物在水稻中的残留检测方法及残留动态.pdfVIP

, 2005, 7( 1): 54258 Ch ine e Journal ofP e ticide Science # 研究论文# * 韩丽君 , 钱传范, 江才鑫, 王武杰 ( , 100094) : ( GC2ECD ) , 2, 4, 62 72. 9%~ 103. 4% , 1. 46% ~ 9. 38% , , 3. 4 d; , 166. 6 mg /L 0. 0250. 056 mg /kg, :; ; ; ; 2, 4, 62 : O657. 7; S481. 8 : A : 100827303(2005) 0 12 00542 05 R esidue Detection and Degradation of Proch loraz and itsM etabolites in R ice * HAN L i2jun , Q IAN Chuan2fan, JIANG Cai2xin, WANG W u2jie (C ollege of Science, China Agr icu ltural Un iver ity, Beijing 100094, China ) Ab stract: Re idue detection and degradation of prochloraz 45% EC and it m etabo lite in rice w ere inve tigated and their re idue w ere determ ined w ith GC2ECD. A fter mi ple clean ing2up of the amp le , proch loraz and it m etabolite reacted w ith the pyridine ch loride at h igh temperature, the product 2, 4, 62trich lorophenolw a then detected. The fortified recoverie of proch lorazw ere 72. 9% ~ 103. 4% , the CV w ere 1. 46% ~ 9. 38% . The re u lt obtained from wt o year expermi en t how ed that the degradation of prochloraz in rice eed ling w a fa t, and it half2life wa on ly 3. 4 day . A fter a grow ing ea on, on ly in the am ple from h igh do age of app lication, the re idue in rice grain and rice traw w ere 0. 025 and 0. 056 m g /kg re pectively, no detectable re iduew a found in the other am ple . K ey words: proch loraz; re idue dynam ic; rice; GC2ECD; 2, 4, 62trich lorophenol [3] ( proch loraz ) , , , ([ 1, 2 ] ) ,