二氧化硅掺杂银复合抗菌颗粒的制备与表征.pdfVIP

第 卷第 期 装 学 报 5 2 Vol.5 No.2 年 月 2013 4 Packaging Journal April 2013 doi:10.3969/j.issn .1674-7 100.20 13.02.001 氧化硅掺杂银复合抗菌颗粒的制备与表征 永 马洪月 赵 红 （齐齐哈尔大学 轻工与纺织学院，黑龙江 齐齐哈尔 161006 ） 摘 要：在二氧化硅形成的过程中，利用硅烷偶联剂KH-550 的特殊结构使银均匀地分布在二氧化硅表 面，然后通过甲醛还原，制得了二氧化硅掺杂银复合抗菌颗粒。并通过扫描电子显微镜、透射电子显微镜 等对所合成的纳米银抗菌材料的形貌进行了表征与分析。结果显示：复合颗粒分散均匀，直径约350 nm ，尺 寸稳定；银颗粒直径约10 nm ，均匀分布在二氧化硅的表面；载银质量分数约为13%。 关键词：银；二氧化硅；复合抗菌颗粒；硅烷偶联剂 中图分类号： 文献标志码： 文章编号： 1674 7100(2013)02 0001 04 O612.4 A - - - Preparation and Characterization of Silica Doped Silver Antibacterial Particles ， ， Li Yong Ma Hongyue Zhao Hong （ ， ， ） College of Light Indu stry and Textile Qiqihar University, Qiqihar Heilongjiang 161006 China ： Abstract The silver and the silica by the special structure of KH-550 were combined. The silver was distributed in silica surface during the formation of silica, and then through the reduction of formaldehyde, silica doped silver antibacterial particles would be got eventually. The formation mechanism of nano-silica doped silver antibacterial particles, combined with SEM、TEM and other means were applied for analysis and characterization . The results showed that the size of compound particle was about 350nm in diameter, and the silver doped on silica surface was about 10nm, and compound particles contained about 13% silver (mass). ： ； ；