葡萄酒和软木塞中2,4,6-三氯苯甲醚检测方法的研究进展.pdfVIP

304 2014, Vol.35, No.15 食品科学 ※专题论述 葡萄酒和软木塞中2,4,6-三氯苯甲醚检测 方法的研究进展 1 2 1,* 2 2 2 张亚莲 ，柳 菡 ，王岁楼 ，李静静 ，沈伟健 ，赵增运 （1.中国药科大学药学院，江苏 南京 210009 ；2.江苏出入境检验检疫局，江苏 南京 210001 ） 摘  要：本文介绍了葡萄酒和软木塞中2,4,6-三氯苯甲醚（2,4,6-trichloroanisole ，TCA ）的来源及影响，分析了 2,4,6-三氯苯甲醚的检测难点，总结了目前检测2,4,6-三氯苯甲醚方法的总体趋势及现状。按照前处理方法的原理分 类，介绍了前处理方法的定义、特点，并概述和讨论了前处理方法在萃取葡萄酒和软木塞中2,4,6-三氯苯甲醚中的 应用；根据仪器检测方法的不同特点，总结和讨论了仪器检测方法在分析检测葡萄酒和软木塞中2,4,6-三氯苯甲醚 的应用。前处理方法和仪器检测方法相结合，达到了浓缩和检测葡萄酒和软木塞中2,4,6-三氯苯甲醚的目的。 关键词：2,4,6-三氯苯甲醚；葡萄酒；软木塞；检测方法 Progress in the Detection of 2,4,6-Trichloroanisole in Wine and Cork Stoppers 1 2 1,* 2 2 2 ZHANG Ya-lian , LIU Han , WANG Sui-lou , LI Jing-jing , SHEN Wei-jian , ZHAO Zeng-yun (1. College of Pharmacy, China Pharmaceutical University, Nanjing 210009, China; 2. Jiangsu Entry-Exit Inspection and Quarantine Bureau, Nanjing 210001, China) Abstract: This article describes the source and impact on the flavor quality of wine of 2,4,6-trichloroanisole (TCA) in wine and cork stoppers, analyzes obstacles to the detection of TCA, and summarizes the currently available analytical methods for TCA in wine and cork stoppers. Sample pretreatment methods are classified by their principles, and their definitions, characteristics and applications for TCA detection in wine and cork stoppers are discussed. Also summarized are the characteristics and applications to detect TCA in wine and cork stoppers of different analytical instruments. To conclude, the combination of extraction techniques and instrumental detection enables the condensation and ana