化学沉淀法与层状液晶法制备纳米乳酸钙.pdfVIP

Abstract The purpose of the present work is to investigate the preparation methods of nanoparticles of calcium lactate, and the prepared samples of calcium lactate meet the specification stipulated in the standard on food grade in order to improve the application efficiency and additional value of calcium lactate. On the basis of comprehensive analysis on the factors to control the formation of calcium lactate nanopowder, the process flowsheets of manufacturing nanopowder were put forward using chemical precipitation method and lamellar liquid crystal method. Lactic acid and calcium hydroxide were selected as raw materials in the two different methods. So far as the chemical precipitation method, the effect of factors such as the ration of calcium hydroxide to lactic acid, operating temperature and stirring speed on the mean size of calcium lactate particle was examined by means of single factor test method, and the appropriate process conditions were determined by multi-factor orthogonal test procedure. With respect to lamellar liquid crystal method, taking the system of Triton X-100/n-C H OH/H O as the templates for lamellar liquid 10 21 2 crystal, the preparation of the nanopowder of calcium lactate was carried out, with water within single phase region for the lamellar liquid crystal replaced by aqueous solution of calcium lactate. The composition and apparent solubility of calcium lactate in lamellar liquid crystal were determined, and the appropriate process conditions were determined by single factor test method. The performance of prepared samples were detected according to corresponding standard with food grade stipulated in China, and the particle size and particle size distribution were measured by multi-angle sub-micro particle size anal