2.8万ta甲苯-乙苯精馏工艺设计【毕业论文】.doc

本科毕业论文 （20 届） 2.8万t/a甲苯-乙苯精馏工艺设；；ABSTRACT This design to separate the Toluene--Ethylbenzene mixture, uses the lamina cribrosatype rectifying tower. When production, raw material fluid preheating enough to after assigning thetemperature enters the feed plate unceasingly after the pre-heater, with the rectifying section phegma convergence by the board lower reaches, and with the rise vapor intimate contact, carries on the mass transfer and the heat transfer process unceasingly, finally enters reboiler's liquid nearly to feel embarrassed the volatile component, draws out a part delivers the pre-heater recycling partial heat energies after the distill residue to escort to the storage tank. The surplus part in the reboiler with the indirect steam heating gasification, the production vapor enters in the tower by the board rise, when every time after together column tray, makes in the vapor the easy volatile component to increase, the difficult volatile component to reduce, after passing through certain column trays, enters the tower to go against the condenser complete condensation, an obtained condensate part makes the phegma, another part after chiller temperature decrease goes against the product as the tower (also saying that distillate) escorts to the storage tank. In the design uses bubble point feeding, the reflux ratio for smallest reflux ratio 2 times. This article the rectifying tower some main design feature carries on the computation regarding this. Key word: Rectifying tower ； Lamina cribrosa paper ； reflux ratio 目录 前 言 5 第一章 生产流程方案确定 6 1.1设计条件 6 1.2生产流程确定和说明 6 1.3生产流程简述 7 第二章 精馏塔的设计 8 2.1设计方案选定 8 2.2精馏塔的物料衡算 11 2.3塔板数的确定 11 2.4塔的操作工艺条件及相关物性数据的计算 14 2.5精馏塔的气、液相负荷计算 20 2.6精馏塔的塔体工艺尺寸计算 21 2.7塔板主要工艺尺寸的计算 22 2.8筛板的流体力学验算 25 2.9塔板负荷性能图 29 2.10、精馏塔的设计计算结果汇总一览表 36 第三章冷凝器的设计 37 3.1、确定设计方案 37 3.2、确定物性数据 37 3.3、热负荷计算 38 3.4逆流平均温差 39 3.5、冷却水用量 40 3.6、估算传热面积 40 3.7换热器的工艺结构尺寸 40 3.8、换热器核算 41 3.9换热器主要结构尺寸和计算结果 44 第四章再沸器的设计 45 4.1有关物性的确定 45 4.2估算传热面积、初选换热器型号 47 4.3传热能力