智能型冷原子荧光测汞仪测定10种中药材中痕量汞_药学论文.docVIP

智能型冷原子荧光测汞仪测定10种中药材中痕量汞_药学论文 智能型冷原子荧光测汞仪测定10种中药材中痕量汞_药学论文 作者：李平，胡广林，罗盛旭，张岐 【摘要】 　　目的 测定海南产中药材中重金属汞的含量水平并对其潜在健康风险进行分析。方法采用高压密封消解-冷原子荧光光谱法，对海南产10种中药材巴戟天、胡椒根、灵芝、砂仁、益智、槟榔、广藿香、珍珠、海藻、海马中汞含量进行了测定。结果海南产10种中药材样品中汞含量处于0.006 1～0.066 μg·g-1之间，且都小于0.20 μg·g-1。结论所有受检样品汞含量指标均符合中国商务部《药用植物及制剂进出口绿色行业标准》（WM/T2-2004）要求，海南产中药材汞的健康风险性低 【关键词】 汞； 智能型冷原子荧光测汞仪； 中药材 　　Abstract:ObjectiveTo estimate the potential healthy risk of mercury from ten kinds of traditional Chinese medicinal materias produced in Hainan Island of China, including Morinba officinalis How, Piper nigrum L., Genoderma lucidum Karst, Amomum villosum Lour., Alpinia oxyphylla Miq., Areca catechu L., Pogostemon cablin Benth, Pteria martensii Dunker, Sargassum pallidum C.Ag. and Hippocoampus kelloggi Jordan et Snyder. MethodsCold vapor atomic fluorescence spectrometry combined with pressurized sample digestion was used to determine the contents. ResultsThe determination results（n=8）of mercury for 10 kinds of TCMs were Morinba officinalis How, 0.021 μg·g-1; Piper nigrum L., 0.066 μg·g-1; Genoderma lucidum Karst, 0.027 μg·g-1; Amomum villosum Lour., 0.023 μg·g-1; Alpinia oxyphylla Miq., 0.017 μg·g-1; Areca catechu L., 0.034 μg·g-1; Pogostemon cablin Benth., 0.006 1 μg·g-1; Pteria martensii Dunker, 0.017 μg·g-1; Sargassum pallidum C.Ag., 0.014 μg·g-1; Hippocoampus kelloggi Jordan et Snyder, 0.028 μg·g-1,and all data were lower than 0.20 μg·g-1. ConclusionThe data revealed that mercury contents for all the test samples of the above-mentioned 10 medicinal materias meet the requirement listed in Green Trade Standards of Importing amp; Exporting Medicinal plants amp; Preparations (WM/T2-2004, China) , and the healthy risk of mercury for 10 kinds of TCMs is low. 　　Key words:Mercury; Intellectualized cold vapor atomic fluorescence mercury analyser; Traditional Chinese medicines 　　中药中重金属成分直接影响其使用安全性，在保障中药有效成分的同时，严格控制其重金属含量非常必要［1,2］。重金属Hg在人体内具有相当高的蓄积毒性，主要表现在对神经系统和肾脏产生不可逆的损害［3］，因此Hg是中药质量检验的必测项目。海南省生态环境优良，非常适合中药材规模化种植［4］。目前，关于海南产中药材中重金属Pb