voc挥发性有机化合物分析方法.docVIP

泉岛公司色谱耗材专家 EPA 8260 Volatiles in Water Application 2432 GC/MS Technique : GC/MS Column : Fused Silica 60m x 0.32mm FactorFour VF-624ms, df=1.8 μm Part no.: CP9105 GC : CP3900 Temperature : 35 oC (2 min), 8 oC/min to 160 oC, 10 oC/min to 200 oC, 20 oC/min to 260 oC 5 min) Carrier gas : Helium, 1.2 mL/min Sampler : Tekmar 3000, purge and trap Injection : Split 1:20, Temp. 230 oC, 5 mL purge Detector : MS, Ion Trap 2100T; Temp. Trap: 150 oC, Temp. Manifold: 40 oC, Temp. Transfer line: 250 oC; Storage level of ms is set to exclude water and methanol ions Sample conc. : 10 ng / component Peak identification, see next page 1 Dichlorodifluoromethane 2 Chloromethane 3 Vinyl chloride 4 Bromomethane 5 Chloroethane 6 Trichlorofluoromethane 7 1,1-Dichloroethene 8 Acetone 9 Carbon disulfide 10 Methylene Chloride 11 Methyl tert-butyl ether (MTBE) 12 trans-1,2-DCE 13 1,1-Dichloroethane 14 2-Butanone 15 cis-1,2-DCE 16 2,2-Dichloropropane 17 Bromochloromethane 18 Chloroform 19 Dibromofluoromethane 20 1,1,1-Trichloroethane 21 1,1-Dichloropropene 22 Carbon Tetrachloride 23 1,2-Dichloroethane-d4 24 Benzene 25 1,2-Dichloroethane (EDC) 26 Benzene, fluoro- 27 Trichloroethene (TCE) 28 1,2-Dichloropropane 29 Dibromomethane 30 Bromodichloromethane 31 cis-1,3-dichloropropene 32 4-Methyl-2-pentanone 33 Toluene-d8 34 Toluene 35 trans-1,3-dichloropropene 36 1,1,2-Trichloroethane 37 Tetrachloroethene (PCE) 38 2-Hexanone 39 1,3-Dichloropropane 40 Dibromochloromethane 41 1,2-Dibromoethane (EDB) 42 Benzene-d5-, chloro- 43 Chlorobenzene 44 Ethylbenzene 45 1,1,1,2-Tetrachloroethane 46 mp-Xylenes 47 o-Xylene 48 Styrene 49 Bromoform 50 Isopropylbenzene 51 4-Bromofluorobenzene 52 1,1,2,2-Tetrachloroethane 53 Bromobenzene 54 1,2,3-Trichloropropane 55 n-Propylbenzene 56 2-Chlorotoluene 57 1,3,5-Trimethylbenzene 58 4-Chlorotoluene 59 tert-Butylbenzene 60 Toluene, p-isopropyl 61 1,2,4-Trimethylbenzene 62 sec-Butylbenzene 63 1,3-Dichlorobenzene 64 1,4-Dichlorobenzene-d4 65 1,4-Dichlo