CdSe纳米晶的制备及性能表征.pdfVIP

14 1 2003 1 J our nal of Op toelectronics Laser Vol. 14 No. 1Jan. 2003 CdSe 纳米晶的制备及性能表征 刘舒曼, 徐　征, Wageh S. , 徐叙王容 ( , , 100044) : ( RSH) , CdSe , 1. 84. 0 nm -X-(XRD) (T EM ) ( HRT EM) ; , , : CdSe; ; ; : TN304:A : 100 -0086(2003) 01-0046-04 Synthesis and Characterization of CdSe Nanocrystals LIU Shu-man, XU Zheng, W ageh S. , XU Xu-rong ( , , , Institute of Optoelectronic Technology Laboratory of Information St orage Display and Materials Northern Jiaotong University , Beijing 100044, China) Abstract : CdSe nanoparticles were synthesized in aqueous solution by using mercapto-acetate acide as stabilizer. Nanosized particles withthe narrow size-dispersionfrom 1. 8 nmto 4.0 nmwere obtained by . - , - selectively precipitation The nanoparticles were characterized by UV vis absorption spectra X ray ( ) , ( ) ( ) . powder diffraction XR transmission electron microscopy TEM and high resolution TEM HRTEM Well dispersed nanoparticles were observed under HRTEM only in the case that surfactants were as- sembled on surfaces of the nanoparticles, which indicatedthat suchassembly of surfactants onsurfaces - . of nanoparticles was a effective method to obtainwell dispersed particles inorganic solution : ; ; ; Key words CdSe nanoparticles synthesis aqueous solution ( % ) , 1