毕业设计（论文）-碱溶粉煤灰提取硅工艺条件的优化.docVIP

攀枝花学院本科毕业论文 碱溶粉煤灰提取硅工艺条件的优化 学生姓名： 学生学号： 200810903041 院（系）： 攀枝花学院生化系 年级专业： 08级环境工程 指导教师： 二〇一二年五月  摘 要 本文主要以攀枝花的粉煤灰为基本材料,参照碱溶粉煤灰提取硅工艺条件优化，提出碱溶粉煤灰提取二氧化硅工艺，并通过控制各条件达到二氧化硅提取条件的优化。通过单因素实验对粉煤灰粒度，NaOH初始浓度、液固比、碱溶时间、反应温度各因素对粉煤灰提取的影响，又通过正交试验考察制备条件NaOH初始浓度、液固比、碱溶时间、反应温度各因素对氧化硅提取的影响，并确定最优条件组确定最优方案,并确定影响硅提取率各因素的强弱。 结果表明：通过单因素实验，单因素实验结果表明，粉煤灰的粒度对SiO2溶出率影响很大。但粒度达到200目以上时，溶出率变化不大。以研磨后200目粉煤灰在碱浓度为17mol/l、液固比1.5:1、反应温度为130℃、反应时间为6min，可使攀枝花粉煤灰的二氧化硅的溶出率达到最高，并确定影响硅的提取率各因素的强弱顺序为：反应温度NaOH初始浓度固液比反应时间。用此法处理粉煤灰提取硅，具有节能降耗的优点，为粉煤灰的开发与利用开辟了一条新途径。 关键词 粉煤灰，二氧化硅，碱溶法  ABSTRACT This paper mainly to Panzhihua fly ash as basic material, with reference to aluminum fly ash technology principle, put fly ash in alkaline solution extraction silica process, and by controlling the conditions to achieve silica extraction condition optimization.through the single factor experiment on fly ash particle size, initial NaOH concentration, liquid solid ratio, reaction temperature, alkali dissolution time of each factor on fly ash effect of extraction, was investigated through orthogonal test conditions for preparation of initial NaOH concentration, liquid solid ratio, reaction temperature, alkali dissolution time of each factor on silicon oxide extraction effects, and determination of the optimal conditions for determining the optimal solution set. And the study of leaching process and dynamics experiment. The results showed that: through the single factor experiment, single factor experiment results show that, the particle size of fly ash on SiO2dissolution rate influence. But size up to more than 200 eyes, the dissolution rate of change. In200eyes after grinding fly ash in alkaline concentration is 17mol / L, liquid solid ratio of 1.8:1and130 degrees C, reaction 6min, can make the silica dissolution rate reached the highest. And to determine the effect of silicon extraction rate of each factor strength order: reaction temperature NaOH initial concentration