应用电感耦合等离子体质谱法快速检测葡萄酒中57种矿质元素.pdfVIP

应用电感耦合等离子体质谱法快速检测 葡萄酒中57种矿质元素※ 杨玉梅1，杜慧娟1，李伟2，潘秋红¨ (1．中国农业大学食品科学与营养工程学院，北京100083； 2．中粮集团华夏长城葡萄酒有限公司，河北昌黎066600) 用该法检测了酒精发酵结束后的霞多丽、西拉和美乐3个单品种酒中矿质元素含量，结果显示，3个单品种 异，葡萄酒中主要的重金属锌(Zn)、砷(As)、铅(Pb)、镉(Cd)均低于OW的限量。 关键词：电感耦合等离子体质谱；葡萄酒；矿质元素 中图分类号：0657．63 文献标识码：A Quickdeterminationof57mineralelementsinwines byInductivelyCoupled PlasmaMass Spectrometry(ICP-MS) YangYumeil，DuHuiju柚’，LiWei2，Pan Qiuhon91+ ofFoodScienceandNutritional 100083； (1．College Engineering，ChinaAgriculturalUniversity,Beijing 2．HuaxiaGreatWallWine Co．LTD．COFCO，Changli，Hebei066000) Abstract：：Tominimizetheinterferenceof wine onmineraldetermination，aRose complexingredients Honeywine(vitis vinifera，L．)withlowlevelsofmineralelementswasusedasasolventto thestandardsolutions。andwine very prepare samples werediluted onwhichanewmethodofICP．MSwas forsimultaneous analyzed by5％(v／v)nitricacid,based developed determining 57mineralelementsinwines．Underthe conditions．thedetectionlimitsof57elementswereinthe of optimumanalytic range relativestandard than the lower5．00％，andrecoveriesin 0．002(B)～23．10ng／L(Se)，thedeviations(RSD)was ranged allofthemcouldbesuitabletoasimultaneous ofmulti-elementsin 81．15％～108．6％．and determination wines．T