微波辅助固相微萃取联用技术萃取腊肉中多环芳烃的研究.pdfVIP

王艺技求———————瓦丽而矿』幽 微波辅助一固相微萃取联用技术 陈代武，王芳，蒙松年，李绿冰 (邵阳医学高等专科学校药学系，湖南邵阳422000) 摘要：通过比较不同提取方法对多环芳烃(PHAs)的提取效率，建立了腊肉中多环芳烃的微波辅助一固相微萃取联用 16种多环芳烃化合物的优点，适合于腊肉中多环芳烃化合物的分析测定。 关键词：微波辅助一固相微萃取联用技术，气相色谱，多环芳烃，腊肉 onextractionof aromatic frOm Study polycyciic hydrocarbons smokedmeatMAE-SPME by CHEN Dai一唧，WANG Fang，MENGSong—nlan，LILv-bing of Medical (Department 422000，China) Pharmaceuticals，ShaoyangCollege，Shaoyang establishedamethodforthedeterminationof aromatic smoked Abstract：To polycyclic hydrocarbons(PAHs)in meatthe ofmicrowaveassisted by technology extraction(MAE)andsolid-phase theinfluenceofextractionwithmicrowaveassisted chromatography(GC)，andcomparing extraction(MAE)， microwaveassisted kindof extraction(MAE)andsolid—phasemicro—extraction(SPME)，soxhletsextraction，16 i13 were and PAHsthe the method．Therecoveriedofthemethod samplesseparatedquantifiedby proposed frOm78．8％一101．2％andtherelativestandarddeviationswere methodiS ranged 2．5％一6．1％．This sensitive． accurateandsuitabletothedeterminationofPHAsinsmokedmeaL assisted WOrds：microwave Key extraction(MAE)andsolid—phase aromatic meat chromatography(GC)；polycyclichydrocarbons(PAHs)；smoked 中图分类号：TS251．1 文献标识码：A 文章编号：1002—0306(2008)06—0197—04 aromatic 多