乙酰丙酮荧光分光光度法测定环境空气中的微量甲醛_陈炎.pdfVIP

16 4 Vol. 16 No. 4 2000 8 Environm ntal Monitoring in ChinaAu g. 2000 陈　炎, 孙东红, 李　舒, 王　军　　( , 450004) : 建立了乙酰丙酮荧光分光光度法测定空气中微量甲醛 方法, 选择了最佳实验条件, 考察了多种共存物 影响 及最大允许量。该方法最低检出限为0. 0034Lg/ m l, 相对标准偏差为5. 6% , 测定空气中甲醛 最低浓度为0. 0057mg/ m3, 可满足室内外环境空气中甲醛本底及受甲醛污染环境 监测。 : 甲醛; 乙酰丙酮; 荧光分光光度法 : X 832: A : 1002-6002( 2000) 04-0030-03 Determining the trace formaldehyde in air by acetylaceptone fluorephotometry CHEN Y an, t al( H nan Provinc Environm ntal Monitoring C ntr , Zh ngzhou 450004, China) : , Abstract By s l cting th b st xp rim ntal condition and s v ring th influ nc of th co xist s this pap r builds th m thod of d t rmining th trac formald hy d in air by ac tylac pt on fluor photom try. Th limit of d t ction of this 0. 0034 / . 5. 6% , m thod is Lg ml Th r lativ standard d viation is th low st d t ctiv conc nt rat ion of formald hy d in 3 air is 0. 0057mg/ m . T his m thod could d t rmin th formald hyd in background and pollut d air , by formald hy d . : ; ; Key words formald hyd ac tylac pton fluor phot om try , , , , 1 , 1963 B lman[ 1] , 1983 Bisgaard 1. 1 , RF-540 ; KB-6A ; pHS-2 : 415 ; 508 : 32; , EX nm EM nm Ordindt X , Abscissa: X2; Exslit : 5nm ; Emslit : 10nm ; S nsitiv : High , : , , 3, 5 , GPS , , ; , , ( ) , , ( ) ,