三草酸合铁酸钾制备及结构表征.docVIP

三草酸合铁（Ⅲ）酸钾的制备及结构表征 摘要：本次实验用三氯化铁与草酸钾在一定条件下直接配合制备亮绿色晶体三草酸合铁 (Ⅲ)酸钾 ,合成方法简便 ,反应条件易控制 ,产物纯度高 ,用热分析和磁化率测定方法对所合成的配合物结构组成进行测定 ,得有关测定数据与理论值相吻合。[ 1 ] 关键词：三草酸合铁(Ⅲ)酸钾；结晶；配合物；配体；磁化率 Third Oxalate Fe(Ⅲ) Preparation and Nature of Sructure Abstract:In this experiment the bright green crystal of potassium ferrioxalate synthesized under certain surroundings with ferric chloride and potassium oxalate is of high pureness.The method is simple and the conditions are easy to control.From the results of potassium permanganate and magnetize,we get figures accorded exactly with the theoretical ones. Keywords:Third Oxal