匙羹藤总皂甙β环糊精包合物的制备工艺.pdfVIP

2010年5月 基础研究 食品研究与开发 第31卷第5期 匙羹藤总皂甙一13一环糊精包合物的制备工艺 侯会绒1,2。孙兆远1，吴向阳妒，赵婷3，仰榴青3 江苏镇江212013) 摘要：研究匙羹藤总皂甙与is-环糊精包合物的制备工艺。采用饱和水溶液法，在单因素试验的基础上，通过正交试 验，考察投料比、包合温度、包合时间对包合物收率和包合卒的影响。最佳包合条件为：is一环糊精与匙羹藤总皂甙比 例l：l，包合温度50℃，包合时间3h。该制备工艺稳定，可用于匙羹藤总皂甙一B一环糊精包合物的制备。 关键词：匙羹藤总皂甙；Is-环糊精；包合物 oftheInclusion ofTotal from with SaponiusGymenmasylvestreg6一Cyclodextrin Prepatation Compound HOU Hui-ron91”，SUNZhao—yuan‘，WUXiang-yangz‘，ZHAOTin93，YANGLiu-qin93 Food of andChemical Science (1．Jiangsu College，Huai’an223003，Jiangsu，China；2．SchoolChemistry Engineering， of 212013， Pharmacy，JiangsuUniversity，Zhenjiang JiangsuUniversity，Zhenjiang212013，Jiangsu，China；3．School Jiangsu，China) Abstract：Totheinclusion of oftotal in study compoundpreparationtechnologysaponinsGymnemasylvestre with the of basisof factor inclusion methodsaturatedsolution，onthe 13-eyclodextrin．By single experiment，the andinclusionratioofthetotal in in inclusion wereuseda8 recovery Gymnema compounds saponins sylvestre criteriainthe the conditionwas withthe experiment。andoptimulpreparation given IJ9(33)orthogonalexperiment． The conditionwas：theratioof andtotal in was optimumpreparation 13-cyclodextrinsaponinsGymnemasylvestre timewas3hours．The was coul