E用GC和GCMS分析糖类衍生物.pdfVIP

G Model CHROMB-17124; No. of Pages 15 ARTICLE IN PRESS Journal of Chromatography B, xxx (2010) xxx–xxx Contents lists available at ScienceDirect Journal of Chromatography B j o u rn al h omepage: w w w. elsev /locate/chro mb Review Derivatization of carbohydrates for GC and GC–MS analyses A.I. Ruiz-Matute a , O. Hernández-Hernández b , S. Rodríguez-Sánchez b , M.L. Sanz b , I. Martínez-Castro b,∗ a Instituto de Fermentaciones Industriales-CIAL (CSIC), Juan de la Cierva 3, 28006 Madrid, Spain b Instituto de Química Orgánica General (CSIC), Juan de la Cierva 3, 28006 Madrid, Spain a r t i c l e i n f o a b s t r a c t Article history: GC and GC–MS are excellent techniques for the analysis of carbohydrates; nevertheless the preparation Received 15 July 2010 of adequate derivatives is necessary. The different functional groups that can be found and the diversity Accepted 8 November 2010 of samples require specific methods. This review aims to collect the most important methodologies cur- Available online xxx rently used, either published as new procedures or as new applications, for the analysis of carbohydrates. A high diversity of compounds with diverse functionalities has been selected: neutral carbohydrates Keywords: