电铸制备SiC颗粒增强镍基复合材料的工艺与性能.pdf

33 1 机 械 工 程 材 料 Vol. 33 No. 1 2009 1 Materials for Mechanical Engineering Jan. 2009 SiC , , , ( 上海交通大学金属基复合材料国家重点实验室, 上海200030) : 采用电铸技术( 氨基磺酸镍电铸液) 功制备了SiC 颗粒增强镍基复合材料; 用Leica Qwin 图形分析软件和显微硬度计分析了电铸工艺参数对SiC 颗粒增强镍基复合材料中SiC 颗粒 含量以及SiC 含量对该复合材料显微硬度的影响; 用场发射扫描电镜分析了复合材料的截面形貌 - 1 - 2 和SiC 分布结果表明:在 SiC 加入量50 g L 电流密度3 A dm 和磁力搅拌强度 1. 5 次/ min 条件下, 复合材料中SiC 颗粒体积分数达到最高值27% , 其显微硬度值也最高, 为710 HV : 电铸; SiC 颗粒增强镍基复合材料; 显微硬度 : Q153.4 : A : 2009) Electroforming Preparation and Properties of Ni/SiC Composites SHEN Bin, LIU Lei, DENG Yida, HU Wen in ( Shanghai Jiaotong University, Shanghai 200030, China) A stract: Electroforming t echnology w as used to prepare Ni/ SiC composites in the nickel sulphamate bath wit h SiC as reinforcing particles. he effects of process paramet ers on SiC content in Ni/ SiC com posites were investigated by means of Leica Qwin graphics analysis software. he eff ects of particle content in composites on microhardness w ere also analyzed by microhardness instrument. FESEM was used to observe the section surfaces and the distribut ion of SiC in the composites. he results showed that the maximum volume fraction of SiC in Ni/ SiC com posites w as 27% under the conditions of current density of 3 A dm- 2 , particle concentration of 50 g L- 1 and agitation rate of 1. 5 t ime/ min. In addition, the maximum composites microhardness w as 710 HV. Key words: electroforming; Ni/ SiC composite; microhardness Ni/ SiCNiAl2 O3 CuSiC, CuAl2 O3[ 3- 5] 0 , , ( PRMMCs) , , , , , [