FeCoNi合金超细粉体的制备及其微波性能研究.pdf

FeCoNi合金超细粉体的制备及其微波性能研究 曾国勋h2。张海燕h2，葛鹰1。陈易明1 (1．广东工业大学，广州510006；2．毫米波国家重点实验室，南京210096) 的形貌，用激光粒度分析仪测试粉体的粒度，结果显示：合金粉体呈现片状和针状，粒度分布很宽。将制备的合金 粉与石蜡按质量比80：20混合制成样品，在0．5--．8GHZ内，采用矢量网络分析仪测试样品的电磁参数。研究结 果显示：舍金粉体∥’≥2的频率至少高于3GHz，有的达到6GHz；样品的磁导率虚部曲线呈现多模共振的形式。 dB吸波频宽可达5．91GHz(2．09～8 材料反射率计算显示，合金粉的5 GHz)。 [关键词]铁磁合金；超细粉；电磁参数；反射率 [中图分类号]TB34 [文献标识码]A Fabricationand of FeCoNiFinePowders Absorption Alloy ZENGGuo-xunl～，ZHANG2，GE Hai-yanhYin91，CHEN Yi-min91 of (1．GuangdongUniversityTechnology，Guangzhou510006。China； 2．State ofMillimeter KeyLaboratory 210096，China) Waves，Nanjing ofFeCoNiwith [Abstract]Fine differentnominalCo，Nicontentwere citricnitrate powders preparedby sol—gel in methodandthermaltreatment and sizesof were hydrogenatmosphere．Themorphologyparticle samples SEMandlaser size resultsshowthatFeCoNi haveaneedle-like(or by particleanalyzer．The powders withawide sizedisturbution．Andtheobtained were at particle powders in amassratioof randomlydispersedparaffin 80：20formicrowave testinthe Of0．5～8GHz．The of electromagneticparameters frequencyrange frequenciessamples areatleast3GHz，forcertain evenas as6GHz．The of whose／1’≥2 samples high imaginarycomplexpermeabili—