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NiFe2O4尖晶石涂层用纳米Ni-Fe合金的电沉积制备与表征.pdf
Trans. Nonferrous Met. Soc. China 25(2015) 146−153
Fabrication and characterization of electrodeposited nanocrystalline
Ni−Fe alloys for NiFe O spinel coatings
2 4
1,2 2 1 2 2
Li MA , Long ZHANG , Xiao-bing LI , Zhi-you LI , Ke-chao ZHOU
1. School of Metallurgy and Environment, Central South University, Changsha 410083, China;
2. State Key Laboratory of Powder Metallurgy, Central South University, Changsha 410083, China
Received 27 April 2013; accepted 21 November 2014
Abstract: Nanocrystalline Ni−Fe FCC alloy coatings with Fe content of 1.3%−39% (mass fraction) were fabricated on the nickel
substrates using a DC electrodeposition technique. The crystal structure, lattice strain, grain size and lattice constant of the Ni−Fe
alloy coatings were studied by X-ray diffraction technique. The chemical composition and surface morphology of the FCC Ni−Fe
alloy coatings were investigated with the energy dispersive X-ray spectroscopy (EDS) and atomic force microscopy (AFM). The
results show that the Fe content of the Ni−Fe alloy coatings has a great influence on the preferred orientation, grain size, lattice
constant and lattice strain. FCC Ni−Fe alloy coatings exhibit preferred orientations of (200) or (200)(111). With an increase of Fe
content, the preferred growth orientation of (200) plane is weakened gradually, while the preferred growth orientation of (111)
increases. An increase of the Fe content in the range of 1.3%−25% (mass fraction) results in a significant grai
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