单塔精馏系统用户手册.pdfVIP

单塔精馏 使 用 手 册 （教师/ 学员） 单塔精馏单元使用手册 目 录 一， 工艺原理简述 ·····································································2 二， 工艺流程简介 ·····································································2 三， 设备列表············································································3 四，仪表列表············································································3 五， 现场阀列表·········································································4 六， 物料平衡和工艺卡片 ····························································5 七， 复杂控制说明 ·····································································6 八， 操作规程············································································7 （一）装置冷态开车过程··································································7 （二）正常运行··············································································8 （三）正常停车··············································································9 （四）特定事故 ·············································································10 （五）项目列表·············································································13 九， 单塔精馏PID 图········································错误!未定义书签。 十， 单塔精馏DCS 图··········································错误!未定义书签。 北京东方仿真控制技术有限公司 E-mail: service@ 1 电话：01064927568 网 址: 单塔精馏单元使用手册 一，工艺原理简述 精馏是化工生产中分离互溶液体混合物的典型单元操作，其实质是多级蒸馏，即在 一定压力下，利用互溶液体混合物各组分的沸点或者饱和蒸汽压不同，使轻组分（沸点 较低或饱和蒸汽压较高的组分）汽化，经多次部分液相汽化和部分气相冷凝，使气相中 的轻组分和液相中的重组分浓度逐渐升高，从而实现分离。 进料板为界，上部为精馏段，下部为提馏段。一定温度和压力的料液进入精馏塔后， 轻组分在精馏段逐渐浓缩，离开塔顶后全部冷凝进入回流罐，一部分作为塔顶产品（也 叫馏出液），另一部分被送入塔内作为回流液。回流