《Effect of flow field distribution on the synthesis of submicron ZSM5 molecular sieve in a quasisolid system》.pdfVIP
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120
DOI
Effectofflowfielddistributiononthe
synthesis
ofsub.micronZSM.5molecularsievein
aquasi--solid
system
Xia andDouTa01,2术
Zhil,Hu Huan2,Li
Si2,Zhang Xiaofen91,GongYanjun2
Shanxi
。TaiyuanUniversityofTechnology,Taiyuan030024,China
2China 102249,China
UniversityofPetroleum,Beijing
◎China ofPetroleum Berlin 2013
University rBeijing)andSpringer-VerlagHeidelberg
Abstract:Scale—uDofsub—micronZSM.5molecularsieveina was
synthesis quasi.solidsystem
with
traditional ina has
investigated.Comparedhydrothermalsynthesis.thesynthesisquasi.solidsystem
the of time.10w aswellaslowemissions.
crystallization
advantageshighyield.short energyconsumption
solidcontentinthe cancausethemassandheattransfer
However,the
high quasi—solidsystem problems
andmakescalable difficult.Inordertosolvethe have amethodforthe
production problem.wedeveloped
the and
of mass heat thismethodonecan theflowfieldinthereactor
optimization transfer.By vary by
thestirrer ofthesub.micronZSM.5molecularsieveina
changing speed.Scale.uDsynthesis quasi—solid
wascarriedina5L
out reactorwithdouble was
system propeller-typeagitators.Theprocessinvestigated
with characterizationdiffra
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